Manufacture of multinitrated caged molecules for explosives.
3,7,9-Trinitronoradamantane is prepd. from a starting raw material mixt. comprising 9,9-dimethoxybicyclo(3,3,1)nonan-3,7-dione, redistd. pyridine, MeOH, and hydroxylamine hydrochloride through step-process. The multinitrated caged compd. is highly strained and energetic.
|Author:||Walter W. Zajac|
|Location of Patent Registration:||U.S.|